BREAD, MACARONI , PASTA AND BAKER’S WARES

07 Bread, macaroni, pasta and baker's wares
ORGANOLEPTIC TEST
BREAD AND PASTRY – Weight, shape, surface, color, smell, condition of the crumb, crust thickness, taste, consistency, crispiness, appearanceBDS 3412, item2.1, item2.2
Bread ropiness - macroscopicallyBDS 3412, item2.1
PASTA – Appearance and shape, size, color, smell, taste, splitting, crispiness, conditions after boilingBDS 5, item3
PHYSICO-CHEMICAL AND BIOCHEMICAL TESTS
Active acidity (рН) QOP 504-1-FH-26
Titrable (free acidity) by NeumannBDS 3412 item3.3
Water content/dry matterBDS 3412 item3.1;item3.2
Fat content (crude fat) - extractiveBDS 3412 item3.7.4
Protein content (protein, nitrogen)BDS 3412 item3.9
Sugars content (sucrose, lactose, reducing sugars/invert sugar)BDS 3412 item3.6.2
Carbohydrates contentQOP 504-1-FH-41
Crude cellulose content (fibers)BDS ISO 5498; BDS ISO 6541
Ash content - insoluble ash BDS 754 item7.4
Ash contentBDS 754 item7.3; BDS EN ISO 2171
Table salt content /sodium chlorideBDS 3412 item3.4; QOP 504-1-FH-03
Energy valueчл. 10 от Наредба №23/2009
Content of ascorbic acid (Vitamin C)BDS 11812 item2; QOP 504-1-FH-45
Testing for presence of epihydrin aldehyde through Kreis reaction (Fat rancidity)QOP 504-1-FH-30
Determination of peroxide value BDS EN ISO 3960; BDS EN ISO 27107
Potassium sorbate contentBDS 11712 item2
Aluminum contentQOP 504-1-FH-07; BDS EN 15763
Arsenic contentQOP 504-1-FH-19; BDS EN 15763
Iron contentQOP 504-1-FH-02
Mercury contentBDS EN 15763
Iodine contentQOP 504-1-FH-46
Cadmium contentQOP 504-1-FH-17; BDS EN 15763
Tin contentQOP 504-1-FH- 57
Calcium contentQOP 504-1-FH-21
Magnesium contentQOP 504-1-FH-52
Manganese contentQOP 504-1-FH-04
Copper contentQOP 504-1-FH-18
Sodium contentQOP 504-1 ICP/MS-02
Nickel contentQOP 504-1-FH-24
Nitrates contentQOP 504-1-FH-08
Lead contentQOP 504-1-FH-16; BDS EN 15763
Phosphates (phosphorus) contentQOP 504-1-FH-06
Chromium content QOP 504-1-FH-25
Zinc contentQOP 504-1-FH-23
Aflatoxin В1 contentQOP 504-1-FH-20
Aflatoxines В1+В2+G1+G2 (total)QOP 504-1-FH-34
Deoxynivalenol /DON/ contentQOP 504-1-FH-35
Zearalenone contentQOP 504-1-FH-36
Ochratoxin contentQOP 504-1-FH-38
Т2 toxin contentQOP 504-1-FH-39
Fumonisin contentQOP 504-1-FH-37
PorosityBDS 3412 item3.5
Potassium contentQOP 504-1 ICP/MS-01
Content of pesticide: Chlororganic Phosphororganic Nitrogen and sulfur-containingBDS EN ISO 15662
Colorings content:
Yellow:
- Sunset YellowQOP 504-1-IM-HPLC-01
- tartrazineQOP 504-1-IM-HPLC-01
Red:
- erythrosineQOP 504-1-IM-HPLC-01
- azorubineQOP 504-1-IM-HPLC-01
- allura redQOP 504-1-IM-HPLC-01
- ponceauQOP 504-1-IM-HPLC-01
- amaranthQOP 504-1-IM-HPLC-01
Blue
- indigotineQOP 504-1-IM-HPLC-01
- Brillian BlueQOP 504-1-IM-HPLC-01
- Patent BlueQOP 504-1-IM-HPLC-01
Content of saturated fatty acidsBDS EN ISO 12966-2+BDS EN ISO 5508
Content of unsaturated fatty acidsBDS EN ISO 12966-2+BDS EN ISO 5508
MICROBIOLOGICAL TESTS
Total number of microorganisms, including mesophilic aerobes and facultative anaerobes BDS ЕN ISO 4833-1; BDS ЕN ISO 4833-2
Bacillus species including Bacillus CereusBDS EN ISO 21871 item9.1; item9.2; BDS EN ISO 7932
Bacillus species including Bacillus subtilis (var. mesentericus – bread ropiness)BDS EN ISO 21871 item9.1; item9.2; BDS EN ISO 7932
Water activityISO 21807
YeastBDS ISO 21527-1; -2
Escherichia coliISO 16649-2; ISO 7251 item9.1; item9.2
Escherichia coli O157BDS EN ISO 16654
Enterobacteria, including Proteus, Klebsiella, Citrobacter ISO 21528-1 item9.2; item9.3; ISO 21528-2
Clostridia sulfite-reducingISO 15213
Coagulase-positive staphylococciBDS EN ISO 6888-1+A1;-2+A1;-3+AC item9.1;-3+AC item9.2
ColiformsISO 4831item9.1; item9.2; ISO 4832
LeuconostocCOMECON ST 5806
Listeria monocytogenesBDS EN ISO 11290-1+А1; -2+А1
Mesophilic lactic bacteriaBDS ISO 15214
MouldsBDS ISO 21527-1; -2
Pseudomonas aeruginosaBDS EN ISO 13720
Psychrotrophic microorganismsBDS ISO 17410
Salmonella speciesBDS ЕN ISO 6579; SD СЕN ISO/ TS 6579-2
GENETICALLY MODIFIED ORGANISMS
Determination of presence of genetically modified organisms – 35SBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
Determination of presence of genetically modified organisms – FMVBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
Determination of presence of genetically modified organisms – NOS terminatorBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
09 Dairy products, flours, starch, semolina
ORGANOLEPTIC TEST
Dairy products - Appearance, composition, color, smell, taste, crispiness, impuritiesBDS 754, item6, item8, item10
STARCH – Appearance, composition, color, smell, impuritiesBDS 754 item10
Warehouse pestsBDS 8380, item3, item10
PHYSICO-CHEMICAL AND BIOCHEMICAL TESTS
Active acidity (рН)QOP 504-1-FH-26
Titrable (free acidity)BDS 754 item7.9
Water content/dry matterBDS ISO 711; BDS EN ISO 712; BDS EN ISO 1666
Fat content (extraction)BDS EN ISO 11085; BDS EN ISO 3947
Protein content (protein, nitrogen)BDS ISO 1871; BDS EN ISO 20483; BDS EN ISO 3188;BDS EN ISO 5378
Sugars content (sucrose, lactose, reducing sugars/invert sugar)BDS 7169; BDS 3412 item3.6.2
Carbohydrates contentQOP 504-1-FH-41
Starch content BDS EN ISO 10520
Crude cellulose content (fibers)BDS ISO 5498; BDS ISO 6541
Sulphated ash contentBDS EN ISO 5809
Ash contentBDS EN ISO 3593
Table salt content /sodium chloride QOP 504-1-FH-03; BDS EN ISO 5810
Energy valueчл. 10 от Наредба №23/2009
Content of ascorbic acid (Vitamin C)QOP 504-1-FH-45; BDS 754 item11.2
Sulfur dioxide content (total and free)BDS EN 1185
Formic acid contentBDS 11706
Soy protein contentQOP 504-1-FH-32
Aluminum contentQOP 504-1-FH-07
Arsenic contentQOP 504-1-FH-19; BDS EN 15763
Iron content QOP 504-1-FH-02
Mercury contentBDS EN 15763
Iodine; potassium iodide contentQOP 504-1-FH-46
Cadmium contentQOP 504-1-FH-17; BDS EN 15763
Tin contentQOP 504-1-FH- 57
Calcium contentQOP 504-1-FH-21
Magnesium contentQOP 504-1-FH-52
Manganese contentQOP 504-1-FH-04
Copper contentQOP 504-1-FH-18
Sodium contentQOP 504-1 ICP/MS-02
Nickel contentQOP 504-1-FH-24
Nitrates contentQOP 504-1-FH-08
Lead contentQOP 504-1-FH-16; BDS EN 15763
Phosphates (phosphorus) contentQOP 504-1-FH-06
Chromium content QOP 504-1-FH-25
Cyanides content QOP 504-1-FH-53
Zinc contentQOP 504-1-FH-23
Aflatoxin В1 contentQOP 504-1-FH-20
Aflatoxines В1+В2+G1+G2 (total)QOP 504-1-FH-34
Deoxynivalenol /DON/ contentQOP 504-1-FH-35; BDS EN 15791
Zearalenone contentQOP 504-1-FH-36
Ochratoxin contentQOP 504-1-FH-38
Т2 toxin contentQOP 504-1-FH-39
Fumonisin contentQOP 504-1-FH-37
Gluten content:
- wetBDS 13375 item1; BDS EN ISO 21415-1
- dryBDS EN ISO 21415-3
Reduced power and dextrose equivalent in hydrolyzed starch productBDS EN ISO 5377
Acetyl contentBDS EN ISO 11213
Carboxy group content in oxidized starchBDS EN ISO 11214
Carboxymethyl group content in carboxymethyl starchBDS EN ISO 11216
Fatty acidity BDS ISO 7305
Oxyglutin contentBDS 754 item11.1
Content of pesticide: Chlororganic Phosphororganic Nitrogen and sulfur-containingBDS EN ISO 15662
Colorings content:
Yellow:
- Sunset YellowQOP 504-1-IM-HPLC-01
- tartrazineQOP 504-1-IM-HPLC-01
Red:
- erythrosineQOP 504-1-IM-HPLC-01
- azorubineQOP 504-1-IM-HPLC-01
- allura redQOP 504-1-IM-HPLC-01
- ponceauQOP 504-1-IM-HPLC-01
- amaranthQOP 504-1-IM-HPLC-01
Blue
- indigotineQOP 504-1-IM-HPLC-01
- Brillian BlueQOP 504-1-IM-HPLC-01
- Patent BlueQOP 504-1-IM-HPLC-01
Vitamin content:
- А (retinol)BDS EN 12823-1;2
- А (beta-carotine)BDS EN 12823-1;2
- В1 (thiamine)QOP 504-1-IM-LC/MS-02
- В3 (niacin)QOP 504-1-IM-LC/MS-02
- В6 (pyridoxine)QOP 504-1-IM-LC/MS-02
- В7 (biotin/vitamin Н)QOP 504-1-IM-LC/MS-02
- С (ascorbic acid)BDS EN 14130
- D (D2 ergocalciferol)BDS EN 12821
- D (D3 colecalciferol)BDS EN 12821
- Е (tocopherols)BDS EN 12822
- К (phytomenadione)BDS EN 14148
Content of saturated fatty acidsBDS EN ISO 12966-2 + BDS EN ISO 5508
Content of unsaturated fatty acidsBDS EN ISO 12966-2+BDS EN ISO 5508
MICROBIOLOGICAL TESTS
Total number of microorganisms, including mesophilic aerobes and facultative anaerobesBDS ЕN ISO 4833-1 BDS ЕN ISO 4833-2
Bacillus species including Bacillus CereusBDS EN ISO 21871 item9.1;item9.2; BDS EN ISO 7932
Bacillus species including Bacillus subtilis (var. mesentericus)BDS EN ISO 21871 item9.1;item9.2; BDS EN ISO 7932
Water activityISO 21807
YeastBDS ISO 21527-1;-2
Escherichia coliISO 16649-2; ISO 7251 item9.1; item9.2
Escherichia coli O157BDS EN ISO 16654
Enterobacteria, including Proteus, Klebsiella, Citrobacter ISO 21528-1 item9.2; item9.3; ISO 21528-2
Clostridia sulfite-reducing ISO 15213
Coagulase-positive staphylococciBDS EN ISO 6888-1+A1;-2+A1; -3+AC item9.1; item9.2
ColiformsISO 4831item9.1; item9.2; ISO 4832
Listeria monocytogenesBDS EN ISO 11290-1+А1; -2+А1
MouldsBDS ISO 21527-1; BDS ISO 21527-2
Salmonella speciesBDS ЕN ISO 6579; SD СЕN ISO/TS 6579-2
GENETICALLY MODIFIED ORGANISMS
Determination of presence of genetically modified organisms – 35SBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
Determination of presence of genetically modified organisms – FMVBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
Determination of presence of genetically modified organisms – NOS terminatorBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1