CANNED PRODUCTS

13 Canned products (sterilized and pasteurized) of animal origin with/without vegetable additives and UHT food products
ORGANOLEPTIC TEST
BOXES — air-tightness, outer surface, inner surface, bulging, wobbling and vibrating lids and bottoms, shape and sizes; BDS 1035, item3; BDS 7682
CONTENT - appearance /of ingredients, color/, smell, taste, consistency, cross-section surface, foreign impurities
PHYSICO-CHEMICAL AND BIOCHEMICAL TESTS
Active acidity (рН)BDS 11688; BDS 1035 item4.3
Titrable (free acidity) BDS 1035 item 4.5.8; BDS 6996
Water content/dry matter - gravimetricBDS EN 12145
Water content/dry matter - gravimetricBDS 1035 item4.5.2
Water content/dry matter - gravimetricBDS 15437
Water content/dry matter - refractiveBDS 16612
Fat content (extraction)BDS 6997; BDS 1035 item4.5.4
Protein content (protein, nitrogen)BDS 1035 item4.5.3; BDS 14431; BDS 15438
Sugars content (sucrose, lactose, reducing sugars/invert sugar)BDS 7169
Carbohydrates contentQOP 504-1-FH-41
Starch contentBDS 5713
Crude cellulose content (fibers)BDS ISO 5498; BDS ISO 6541
Ash contentBDS 9373
Table salt content /sodium chlorideQOP 504-1-FH-03; BDS 7168 item4; BDS 1035 item 4.5.5
Energy valueчл. 10 от Наредба №23/2009
Content of ascorbic acid (Vitamin C)QOP 504-1-FH-45
Sodium hydroxide residues contentQOP 504-1-FH-15
Chlorine residues contentQOP 504-1-FH-27
Testing for presence of epihydrin aldehyde through Kreis reaction (Fat rancidity)QOP 504-1-FH-30
Vegetable fats presence in milk fat through Bélier reaction QOP 504-1-FH-29
Starch content – quality responseQOP 504-1-FH-28
Determination of peroxide value BDS EN ISO 3960; BDS EN ISO 27107
Benzoic acid content BDS 1554 item III.15
Potassium sorbate contentBDS 11712 item2
Sulphurous acid content BDS 1554 item III.13
Formic acid contentBDS 11706
Soy protein contentQOP 504-1-FH-32
Aluminum contentQOP 504-1-FH-07
Arsenic (presence) contentQOP 504-1-FH-19; BDS 1554 item III.16; BDS EN 15763
Barium contentBDS EN ISO 17294-2
Boron contentBDS EN ISO 17294-2
Iron content QOP 504-1-FH-02
Mercury contentQOP 504-1-FH-61; BDS EN 15763
Iodine contentQOP 504-1-FH-46
Cadmium contentQOP 504-1-FH-17; BDS EN 15763
Tin contentQOP 504-1-FH- 57; BDS EN 15765
Calcium contentQOP 504-1-FH-21
Magnesium contentQOP 504-1-FH-52
Manganese contentQOP 504-1-FH-04
Copper contentQOP 504-1-FH-18
Sodium contentQOP 504-1 ICP/MS-02
Nickel contentQOP 504-1-FH-24
Nitrates contentQOP 504-1-FH-08; BDS 16591
Nitrites contentQOP 504-1-FH-05; BDS 1035
Lead contentQOP 504-1-FH-16; BDS EN 15763
Selenium contentBDS EN ISO 17294
Sulphates contentQOP 504-1-FH-09; BDS EN 1142
Phosphates (phosphorus) contentQOP 504-1-FH-06
Chromium content QOP 504-1-FH-25
Cyanides content QOP 504-1-FH-53
Zinc contentQOP 504-1-FH-23
Aflatoxin M1 contentQOP 504-1-FH-31
Ammonia content according to Nessler methodBDS 1323 item2.3.5
Ammonia content according to Eber’s testBDS 1323 item2.3.6; BDS 9368 item1.8;item5.9;item6.3
Hydrogen sulphideBDS 1323 item 2.3.8; BDS 9368 item1.9; item2.5; item5.10; item6.2
Connective tissue protein (hydroxyproline) contentBDS 14780
Histamine content in 9 unitsQOP 504-1-FH-33
Proportional content of ingredientsBDS 7181 item3; BDS 15359 item2
Net weight determination BDS 7181 item2; BDS 15359 item1
Potassium contentQOP 504-1 ICP/MS-01
Content of pesticide: Chlororganic Phosphororganic Nitrogen and sulfur-containing BDS EN ISO 15662
Sweeteners content:
- acesulfame К BDS EN 12856; BDS EN 15911
- saccharineBDS EN 12856; BDS EN 15911
- aspartameBDS EN 12856; BDS EN 15911
- cyclamateBDS EN 12857;BDS EN 15911
Colorings content:
Yellow:
- Sunset YellowQOP 504-1-IM-HPLC-01
- tartrazineQOP 504-1-IM-HPLC-01
Red:
- erythrosineQOP 504-1-IM-HPLC-01
- azorubineQOP 504-1-IM-HPLC-01
- allura redQOP 504-1-IM-HPLC-01
- ponceauQOP 504-1-IM-HPLC-01
- amaranthQOP 504-1-IM-HPLC-01
Blue
- indigotineQOP 504-1-IM-HPLC-01
- Brillian BlueQOP 504-1-IM-HPLC-01
- Patent BlueQOP 504-1-IM-HPLC-01
Vitamin content:
- А (retinol)BDS EN 12823-1;2
- А (beta-carotine)BDS EN 12823-1;2
- В1 (thiamine)QOP 504-1-IM-LC/MS-02
- В3 (niacin)QOP 504-1-IM-LC/MS-02
- В6 (pyridoxine)QOP 504-1-IM-LC/MS-02
- В7 (biotin/vitamin Н)QOP 504-1-IM-LC/MS-02
- С (ascorbic acid)BDS EN 14130
- D (D2 ergocalciferol)BDS EN 12821
- D (D3 colecalciferol)BDS EN 12821
- Е (tocopherols)BDS EN 12822
- К (phytomenadione)BDS EN 14148
Content of saturated fatty acidsBDS EN ISO 12966-2+BDS EN ISO 5508
Content of unsaturated fatty acidsBDS EN ISO 12966-2+BDS EN ISO 5508
Pharmacological substances residues content:
Antibiotics (Quinolines) – flumequinQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfaguanidinQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfadiazineQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfamerazinQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfamethoxazoleQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfapyridineQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfatiazolQOP 504-1-IM-LC/MS-01
Antibiotics (Sulfonamides) - sulfacetamideQOP 504-1-IM-LC/MS-01
Antibiotics (Tetracyclines) – oxytetracycline хидрохлоридQOP 504-1-IM-LC/MS-01
Antibiotics (Tetracyclines) – tetracycline hydrochlorideQOP 504-1-IM-LC/MS-01
Antibiotics (Tetracyclines) – chlortetracycline hydrochlorideQOP 504-1-IM-LC/MS-01
MICROBIOLOGICAL TESTS
Total number of microorganisms, including mesophilic aerobes and facultative anaerobes BDS 1035 item5.9.1; BDS 6877 item2.3; BDS ЕN ISO 4833-1 BDS ЕN ISO 4833-2
Mesophilic aerobs non-spore-forming microorganismsBDS 1035 item5.9.1; BDS 6877 item2.3.
Mesophilic aerobs - vegetative forms of spore-forming microorganismsBDS 1035 item5.9.1; BDS 6877 item2.3.
Mesophilic aerobs spore forms of saprophytic microorganisms BDS 1035 item5.9.1; BDS 6877 item2.3.
Mesophilic anaerobs microorganismsBDS 1035 item5.9.2; BDS 6877 item2.3.
Mesophilic anaerobs microorganisms - vegetative forms BDS 1035 item5.9.2; BDS 6877 item2.3.
Mesophilic anaerobs microorganisms - spore forms BDS 1035 item5.9.2; BDS 6877 item2.3.
Thermophilic aerobes and facultative anaerobes microorganismsBDS 1035 item5.9.3; BDS 6877 item2.3.
Thermophilic aerobes microorganisms - non-spore-formingBDS 1035 item5.9.3; BDS 6877 item2.3.
Thermophilic aerobes microorganisms - vegetative forms of spore-formingBDS 1035 item5.9.3; BDS 6877 item2.3.
Thermophilic aerobes microorganisms - spore forms of saprophytic BDS 1035 item5.9.3; BDS 6877 item2.3.
Thermophilic anaerobs microorganismsBDS 1035 item5.9.4; BDS 6877 item2.3.
Thermophilic anaerobs microorganisms - vegetative forms BDS 1035 item5.9.4; BDS 6877 item2.3.
Thermophilic anaerobs microorganisms - spore forms BDS 1035 item5.9.4; BDS 6877 item2.3.
Antibiotics and SulfonamidesBDS 1323 item4.3.1
Bacillus species including Bacillus Cereus BDS EN ISO 21871 item 9.1; item9.2;
BDS EN ISO 7932;
BDS 13807
Bifidobacterium speciesISO 29981
Brochothrix thermosphactaBDS ISO 13722
Vibrios (other than Vibrio parahaemolyticus and Vibrio cholerae)ISO/TS 21872-2
Vibrio parahaemolyticus; Vibrio cholerae; Vibrio alginolyticusISO/TS 21872-1
Water activityISO 21807
YeastBDS ISO 21527-1; -2
Escherichia coliISO 16649-2; ISO 7251 item9.1; item9.2
Escherichia coli O157BDS EN ISO 16654
Enterobacter (cronobacter) sakazakiiISO/TS 22964
Enterobacteria, including Proteus, Klebsiella, Citrobacter ISO 21528-1 item9.2; item9.3; ISO 21528-2
Enterococus speciesBDS 14593 item6.11; BDS 14973 item5.4
Yersinia enterocoliticaBDS EN ISO 10273
Campylobacter spp. ISO 10272-1; BDS ISO/TS 10272-2
Clostridia perfringensISO 7937
Clostridia sulfite-reducingISO 15213
Coagulase-positive staphylococciBDS EN ISO 6888-1+A1; -2+A1; -3+AC item9.1; item9.2; BDS 13809
ColiformsISO 4831item9.1; item9.2; ISO 4832
Lactobacillus speciesBDS ISO 7889
Lactobacillus acidophilusISO 20128
Lactobacillus delbrueckii subsp. BulgaricusBDS ISO 9232
LeuconostocCOMECON ST 5806
Lipolytic microorganismsBDS 12334 item7
Listeria monocytogenesBDS EN ISO 11290-1+А1; -2+А1
Mesophilic lactic bacteria BDS ISO 15214
Acetobacter microorganismsBDS 15143 item5.1
MouldsBDS ISO 21527-1; -2
Proteolytic microorganisms BDS 3434 item10.3
Pseudomonas aeruginosaBDS EN ISO 13720
Psychrotrophic microorganismsBDS ISO 17410
Salmonella speciesBDS ЕN ISO 6579; SD СЕN ISO/ TS 6579-2
StreptococciBDS 14593 item6.9
Thermostatic testBDS 1035 item3.4; BDS 6877 item2.1
Halophilic (salt-tolerant) microorganisms BDS 3434 item10.4
GENETICALLY MODIFIED ORGANISMS
Determination of presence of genetically modified organisms – 35SBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
Determination of presence of genetically modified organisms – FMVBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1
Determination of presence of genetically modified organisms – NOS terminatorBDS EN ISO 21569 +A1; BDS EN ISO 21571 +A1